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Reactor Chamber:
XRK-900
The XRK 900 reactor chamber is the only heating chamber on the market specifically designed for X-ray diffraction experiments for studies of solid state and solid state-gas reactions up to 900 °C and 10 bar. It is a unique tool for in-situ X-ray diffraction investigations - unmatched in robustness and performance.
Key Features
Optimal for solid state - gas reactions
- Furnace heater for excellent temperature uniformity in the sample
- Reliable measurement and control of the sample temperature
- Homogeneous flushing and gas flow inside the chamber without dead volumes
Rugged design
- High quality materials for a long working life
- Housing temperature up to 150 °C to avoid condensation of reaction products
- Fits on all common diffractometers
Choice of sample holders
- Different materials, all chemically very resistant
- Optional sample spinning for good diffraction data quality
- Open sample holders for gas extraction through the sample
- Easy exchange of samples
Technical specifications :
Operating temperature | 25 °C to 900 °C |
---|---|
Temperature measurement | NiCr/NiAl thermocouple |
Atmospheres | Vacuum (1mbar), air, inert gas, reactive gas |
Max. housing temperature | 150 °C |
Angle of incidence | 0 to +165° 2Θ |
Max. operating pressure | 1 mbar to 10 bar |
Sample holder material | Stainless steel or glass ceramics |
Sample diameter | max. 14 mm |
Measure geometry | Reflection |